The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 18, 2007

Filed:

May. 10, 2004
Applicants:

Jonathan N. Howarth, Modesto, CA (US);

Michael S. Harvey, Modesto, CA (US);

Inventors:

Jonathan N. Howarth, Modesto, CA (US);

Michael S. Harvey, Modesto, CA (US);

Assignee:
Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
A61K 33/00 (2006.01); A61K 33/04 (2006.01); A61K 33/14 (2006.01); A61K 33/40 (2006.01); A01N 59/00 (2006.01); A01N 59/02 (2006.01); A01N 59/08 (2006.01); A01N 39/00 (2006.01);
U.S. Cl.
CPC ...
Abstract

The invention includes convenient methods of preparing: (1) highly concentrated liquid bromine-containing biocidal solutions, (2) highly concentrated mixed halogen liquid bromine and chlorine-containing biocidal solutions, and (3) high-activity bromine-containing biocidal solids, all having excellent physical and chemical stability. One method yields solutions that have concentrations of bromine in excess of 18% as Br(8% as Cl) in which the mole ratio of hydroxide ion to hydrogen ion source is at least 1.9:1. Another method employs elemental bromine in conjunction with a solid organic or inorganic halogenating agent to yield halogen solutions at concentrations greater than 22.9% as Br(10.2% as Cl). This method can be performed under conditions that exceed the solubility of the active ingredient such that it crystallizes and is recovered as a hydrated or anhydrous salt in good yield.


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