The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 07, 2020

Filed:

Apr. 21, 2017
Applicant:

Roquette Freres, Lestrem, FR;

Inventors:

Hervé Wyart, Cuinchy, FR;

Thomas Lesur, Haubourdin, FR;

Mathias Ibert, La Chapelle d'Armentieres, FR;

Assignee:

ROQUETTE FRERES, Lestrem, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 493/00 (2006.01); C07D 493/04 (2006.01);
U.S. Cl.
CPC ...
C07D 493/04 (2013.01);
Abstract

A process for manufacturing crystals of 1,4:3,6-dianhydrohexitols, by manufacturing a solution of an internal dehydration product of at least one hexitol, distilling the solution, crystallizing, and wherein the crystallization mother liquors undergo a step of evaporative crystallization. Unlike the prior art processes that seek to recycle the crystallization mother liquors, evaporative crystallization economically and efficiently replaces the succession of steps consisting of at least one concentration, then at least one step of purification by distillation, chromatography, or crystallization.


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