The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 22, 2017

Filed:

Aug. 10, 2015
Applicant:

Air Products and Chemicals, Inc., Allentown, PA (US);

Inventors:

Reinaldo Mario Machado, Allentown, PA (US);

Athanasios Georgios Tsirukis, Bethlehem, PA (US);

Christopher L. Hartz, Slatington, PA (US);

James Robert Leenhouts, Blandon, PA (US);

William F. Schulze, Denver, PA (US);

Assignee:

VERSUM MATERIALS US, LLC, Allentown, PA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C25B 1/00 (2006.01); C25B 9/08 (2006.01); C25B 15/02 (2006.01); C25B 9/16 (2006.01); C23C 16/448 (2006.01);
U.S. Cl.
CPC ...
C25B 15/02 (2013.01); C23C 16/4488 (2013.01); C25B 1/00 (2013.01); C25B 9/08 (2013.01); C25B 9/16 (2013.01); Y02E 60/366 (2013.01);
Abstract

This invention is an apparatus and a method for continuously generating a hydride gas of Mwhich is substantially free of oxygen in a divided electrochemical cell. An impermeable partition or a combination of an impermeable partition and a porous diaphragm can be used to divide the electrochemical cell. The divided electrochemical cell has an anode chamber and a cathode chamber, wherein the cathode chamber has a cathode comprising M, the anode chamber has an anode comprising Mand is capable of generating oxygen, an aqueous electrolyte solution comprising a hydroxide MOH partially filling the divided electrochemical cell. Hydride gas generated in the cathode chamber and oxygen generated in the anode chamber are removed through independent outlets. Mcan be selenium, phosphorous, silicon, metal or metal alloy, Mis metal or metal alloy suitable for anionic oxygen generation, and Mis NHor an alkali or alkaline earth metal.


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