The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 25, 2016

Filed:

Oct. 25, 2013
Applicant:

Mitsubishi Gas Chemical Company, Inc., Tokyo, JP;

Inventors:

Masayuki Katagiri, Niigata, JP;

Yuuichi Sugano, Niigata, JP;

Taketo Ikeno, Niigata, JP;

Makoto Tsubuku, Niigata, JP;

Keita Tokuzumi, Niigata, JP;

Kenj Arii, Tokyo, JP;

Takashi Kobayashi, Tokyo, JP;

Masanobu Sogame, Tokyo, JP;

Yoshinori Mabuchi, Tokyo, JP;

Yoshihiro Kato, Tokyo, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01C 3/08 (2006.01); C07C 261/00 (2006.01); C07C 261/02 (2006.01); C01C 3/00 (2006.01); B32B 15/09 (2006.01); B32B 27/36 (2006.01); C08G 8/28 (2006.01); C08G 65/48 (2006.01); C08J 5/04 (2006.01); C08J 5/24 (2006.01); C08L 61/14 (2006.01); C08L 71/00 (2006.01); C09J 161/14 (2006.01); C09J 171/00 (2006.01); C09K 3/10 (2006.01); H05K 1/03 (2006.01);
U.S. Cl.
CPC ...
C07C 261/02 (2013.01); B32B 15/09 (2013.01); B32B 27/36 (2013.01); C01C 3/004 (2013.01); C08G 8/28 (2013.01); C08G 65/48 (2013.01); C08J 5/04 (2013.01); C08J 5/24 (2013.01); C08L 61/14 (2013.01); C08L 71/00 (2013.01); C09J 161/14 (2013.01); C09J 171/00 (2013.01); C09K 3/10 (2013.01); H05K 1/0346 (2013.01); B32B 2260/046 (2013.01); B32B 2457/08 (2013.01); C08G 2190/00 (2013.01); C08J 2361/14 (2013.01); C08J 2371/10 (2013.01); C08L 2203/20 (2013.01);
Abstract

A method for efficiently producing a cyanogen halide with suppressed side effects, and a method for producing a high-purity cyanate ester compound at a high yield includes contacting a halogen molecule with an aqueous solution containing hydrogen cyanide and/or a metal cyanide, so that the hydrogen cyanide and/or the metal cyanide is allowed to react with the halogen molecule in the reaction solution to obtain the cyanogen halide, wherein more than 1 mole of the hydrogen cyanide or the metal cyanide is used based on 1 mole of the halogen molecule, and when an amount of substance of an unreacted hydrogen cyanide or an unreacted metal cyanide is defined as mole (A) and an amount of substance of the generated cyanogen halide is defined as mole (B), the reaction is terminated in a state in which (A):(A)+(B) is between 0.00009:1 and 0.2:1.


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