The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 24, 2016

Filed:

Aug. 07, 2013
Applicant:

Roquette Freres, Lestrem, FR;

Inventors:

Baptiste Boit, Bethune, FR;

Laurent Rossi, Arras, FR;

Assignee:

ROQUETTE FRERES, Lestrem, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/80 (2006.01); C07C 29/86 (2006.01); C07C 29/78 (2006.01); C07C 31/26 (2006.01);
U.S. Cl.
CPC ...
C07C 29/78 (2013.01); C07C 31/26 (2013.01); C07B 2200/13 (2013.01); C07C 29/80 (2013.01); C07C 29/86 (2013.01);
Abstract

A process for producing a composition which is particularly rich in D-mannitol, the latter being present in the form of crystals having a volume average diameter greater than 20 pm, wherein the crystals correspond to a very large extent to the δ polymorph. This process makes use of the evaporative crystallization technique, in which the seeding and then the controlled growth of the crystals is carried out at different evaporation rates. Finally, very pure δ crystals are advantageously obtained, which have a better compressibility than the α and β homologues thereof and which, by virtue of the sizes thereof, result in a powder which is not subject to caking.


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