The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 24, 2015

Filed:

Feb. 19, 2013
Applicants:

John F. Hartwig, Champaign, IL (US);

Hiroyuki Morimoto, Higashi-ku, JP;

Patrick Fier, Berkeley, CA (US);

Inventors:

John F. Hartwig, Champaign, IL (US);

Hiroyuki Morimoto, Higashi-ku, JP;

Patrick Fier, Berkeley, CA (US);

Assignee:

Other;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 17/32 (2006.01); C07C 22/08 (2006.01); C07B 39/00 (2006.01); C07C 17/263 (2006.01); C07C 29/32 (2006.01); C07C 41/30 (2006.01); C07C 41/48 (2006.01); C07C 45/68 (2006.01); C07C 67/293 (2006.01); C07C 67/343 (2006.01); C07C 201/12 (2006.01); C07C 209/68 (2006.01); C07C 231/12 (2006.01); C07C 253/30 (2006.01); C07D 209/10 (2006.01); C07D 213/26 (2006.01); C07D 215/18 (2006.01); C07D 239/54 (2006.01); C07F 1/08 (2006.01); C07C 37/11 (2006.01); C07C 45/63 (2006.01); C07D 209/08 (2006.01); C07D 213/61 (2006.01); C07D 239/22 (2006.01);
U.S. Cl.
CPC ...
C07C 17/32 (2013.01); C07B 39/00 (2013.01); C07C 17/263 (2013.01); C07C 29/32 (2013.01); C07C 37/11 (2013.01); C07C 41/30 (2013.01); C07C 41/48 (2013.01); C07C 45/63 (2013.01); C07C 45/68 (2013.01); C07C 67/293 (2013.01); C07C 67/343 (2013.01); C07C 201/12 (2013.01); C07C 209/68 (2013.01); C07C 231/12 (2013.01); C07C 253/30 (2013.01); C07D 209/08 (2013.01); C07D 209/10 (2013.01); C07D 213/26 (2013.01); C07D 213/61 (2013.01); C07D 215/18 (2013.01); C07D 239/22 (2013.01); C07D 239/54 (2013.01); C07F 1/08 (2013.01); C07C 22/08 (2013.01);
Abstract

A method of forming a fluorinated molecular entity includes reacting in a reaction mixture an aromatic halide, copper, a fluoroalkyl group, and a ligand. The aromatic halide includes an aromatic group and a halogen substituent bonded to the aromatic group. The ligand includes at least one group-V donor selected from phosphorus and an amine. The overall molar ratio of copper to aromatic halide in the reaction mixture is from 0.2 to 3. The method further includes forming a fluoroalkylarene including the aromatic group and the fluoroalkyl group bonded to the aromatic group. A composition, which may be used in the method, consists essentially of copper, the fluoroalkyl group, and the ligand, where the molar ratio of copper to the fluoroalkyl group is approximately 1.


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