The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 17, 2003

Filed:

Mar. 02, 2001
Applicant:
Inventors:

John W. Schaefer, Wilmington, DE (US);

Mark Heyman, Mays Landing, NJ (US);

Assignee:

TA Instruments-Waters LLC, New Castle, DE (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
F25B 1/900 ;
U.S. Cl.
CPC ...
F25B 1/900 ;
Abstract

A liquid nitrogen cooling assembly incorporating a liquid detector which feeds back to control the nitrogen supply is disclosed. A pressure-controlled nitrogen source (e.g., a dewar) feeds liquid nitrogen to a heat exchanger mounted to a differential scanning calorimetry (DSC) cell. The DSC cell is cooled as liquid nitrogen in the heat exchanger contacting the cell is vaporized into nitrogen gas. The exhaust (nitrogen gas and, occasionally, nitrogen liquid) is fed to a liquid detection/evaporator assembly. If liquid nitrogen is detected in the exhaust by the liquid detection/evaporator assembly, an indication is fed back using a liquid detection feedback loop to a pressure control device. The pressure control device reduces the amount of pressure on the nitrogen source in order to eliminate liquid in the exhaust. When there is liquid in the exhaust, the liquid detection/evaporator assembly also collects and vaporizes the exhaust liquid so that it can be properly vented to atmosphere in gas form. When liquid is no longer detected in the exhaust, the pressure control device increases the pressure on the liquid nitrogen source until liquid is detected in the exhaust. Subsequent cycles control pressure in this manner to keep the heat exchanger full of liquid nitrogen.


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