The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 30, 2025

Filed:

Mar. 13, 2019
Applicant:

Amgen Inc., Thousand Oaks, CA (US);

Inventors:

Da Ren, Thousand Oaks, CA (US);

Melissa Sato, Santa Monica, CA (US);

Assignee:

AMGEN INC., Thousand Oaks, CA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G01N 1/00 (2006.01); G01N 1/40 (2006.01); G01N 30/00 (2006.01); G01N 30/04 (2006.01); G01N 30/06 (2006.01); G01N 30/14 (2006.01); G01N 33/68 (2006.01); G01N 30/02 (2006.01);
U.S. Cl.
CPC ...
G01N 1/4044 (2013.01); G01N 1/40 (2013.01); G01N 30/00 (2013.01); G01N 30/04 (2013.01); G01N 30/06 (2013.01); G01N 30/14 (2013.01); G01N 33/6848 (2013.01); C12Y 304/21004 (2013.01); C12Y 304/21037 (2013.01); G01N 2030/027 (2013.01); G01N 2030/067 (2013.01);
Abstract

The disclosed methods are directed to preparing polypeptides for multi-attribute analysis. The polypeptides are optionally denatured, reduced, and/or alkylated before being subjected to a first digestion. Following the first digestion the large and small fragments resulting from the digestion are separated from each other. A second digestion is then performed on the larger of the fragments. All of the fragments from the two digestions are then analyzed chromatographically, electrophoretically, or spectrometrically, or a combination of these methods. The methods are especially useful for the preparation of therapeutic polypeptides for analysis, especially those that are not easily cleaved.


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