The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 03, 2020

Filed:

Jan. 25, 2017
Applicant:

Bma Braunschweigische Maschinenbauanstalt Ag, Braunschweig, DE;

Inventors:

Jens Mahrholz, Braunschweig, DE;

Andreas Lehnberger, Braunschweig, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C13B 30/02 (2011.01); B01D 9/00 (2006.01);
U.S. Cl.
CPC ...
C13B 30/025 (2013.01); B01D 9/0036 (2013.01); B01D 9/0063 (2013.01); C13B 30/027 (2013.01); B01D 2009/0086 (2013.01);
Abstract

A method for obtaining crystals from a mother solution operates such that mother solution is fed into a crystallisation device. Supersaturation of the mother solution is brought about by open and/or closed-loop control of the temperature (□). Seed crystals are added to the mother solution at a seeding point (Sp). The seed crystals are grown as nuclei by continuous closed-loop process control and are finally removed from the method as crystals. They form the product yield. The formation of crystal nuclei in the mother solution is countered by steps in the closed-loop process control. During the closed-loop process control and the crystallisation procedure, the position of the limit (M) of the formation of secondary nuclei is determined using sensors that detect data currently, wherein the position of the limit (M) is established as a value of the concentration (c) and the temperature (□) from these data. This determined position of the limit (M) of the formation of crystal nuclei is used as the basis for the closed-loop process control of the crystallisation.


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