The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 12, 2019

Filed:

Jan. 26, 2018
Applicants:

Rohm and Haas Electronic Materials Llc, Marlborough, MA (US);

Dow Global Technologies Llc, Midland, MI (US);

Inventors:

Liang Chen, Midland, MI (US);

Leslie E. O'Leary, Midland, MI (US);

Zhifeng Bai, Midland, MI (US);

Yuming Lai, Midland, MI (US);

Jake Joo, Somerville, MA (US);

Assignees:

Rohm and Haas Electronic Materials LLC, Marlborough, MA (US);

Dow Global Technologies LLC, Midland, MI (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 27/26 (2006.01); C07C 67/48 (2006.01); C09K 11/02 (2006.01); C09K 11/54 (2006.01); C09K 11/62 (2006.01); C09K 11/70 (2006.01); B01D 15/08 (2006.01); C08F 220/16 (2006.01); C09D 5/22 (2006.01); C09D 5/24 (2006.01); C09D 133/06 (2006.01); C09K 11/88 (2006.01); C08F 220/18 (2006.01); B82Y 20/00 (2011.01); B82Y 40/00 (2011.01); C08K 3/30 (2006.01); C08K 3/32 (2006.01); C08K 9/02 (2006.01); B82Y 30/00 (2011.01);
U.S. Cl.
CPC ...
C09K 11/025 (2013.01); B01D 15/08 (2013.01); C08F 220/16 (2013.01); C08F 220/18 (2013.01); C09D 5/22 (2013.01); C09D 5/24 (2013.01); C09D 133/062 (2013.01); C09K 11/703 (2013.01); C09K 11/883 (2013.01); B82Y 20/00 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01); C07C 27/26 (2013.01); C07C 67/48 (2013.01); C08F 2800/20 (2013.01); C08K 3/30 (2013.01); C08K 3/32 (2013.01); C08K 9/02 (2013.01); C08K 2003/3036 (2013.01); C09K 11/02 (2013.01); C09K 11/54 (2013.01); C09K 11/62 (2013.01); C09K 11/70 (2013.01); Y10S 438/962 (2013.01); Y10S 977/774 (2013.01); Y10S 977/818 (2013.01); Y10S 977/824 (2013.01); Y10S 977/892 (2013.01); Y10S 977/95 (2013.01);
Abstract

The present invention provides methods for making polymerizable monomer compositions comprising purifying a (b) monomer mixture of (i) one or more monomers having at least two polymerizable vinyl groups and (ii) one or more monomers having a single polymerizable vinyl group as part of a (meth)acrylate ester group by any one or more of treating the monomer mixture in an activated porous alumina or silica column, sieve drying the monomer mixture in a vacuum followed by drying over dried molecular sieves having average pore sizes of from 2 to 20 Angstroms, freeze-pump-thaw (FPT) treating by freezing the monomer mixture in a vessel or container to a temperature below −75° C., degassing the monomer mixture by application of vacuum in the range of 10to 10Pa, sealing the vessel or container under vacuum, and thawing the composition to room temperature; and, combining in an inert gas atmosphere the resulting monomer mixture (b) with a composition (a) of quantum dots in dry form or organic solvent solution.


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