The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 28, 2018

Filed:

Feb. 04, 2014
Applicants:

Sulzer Chemtech Ag, Winterthur, CH;

Futerro S.a., Escanaffles, BE;

Inventors:

Manfred Stepanski, Buchs, CH;

Peter Fässler, Allschwil, CH;

Philippe Coszach, Courcelles, BE;

Assignees:

Sulzer Chemtech AG, Winterthur, CH;

Futerro S.A., Escanaffles, BE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D 3/14 (2006.01); C07D 319/12 (2006.01); B01D 9/00 (2006.01); B01D 1/06 (2006.01); B01D 3/02 (2006.01);
U.S. Cl.
CPC ...
B01D 3/14 (2013.01); B01D 1/065 (2013.01); B01D 3/02 (2013.01); B01D 3/143 (2013.01); B01D 3/148 (2013.01); B01D 9/004 (2013.01); B01D 9/0031 (2013.01); C07D 319/12 (2013.01); B01D 2009/0086 (2013.01);
Abstract

The invention relates to a process for purification of a stream containing a cyclic ester of an alpha-hydroxycarboxylic acid of formula (I), wherein each R independently represents hydrogen or an aliphatic hydrocarbon having 1 to 6 carbon atoms comprising the steps of: (a) separating the cyclic ester-containing stream into one or more cyclic ester-containing vapor fractions and one or more cyclic ester-containing liquid fractions; (b) condensing a cyclic ester-containing vaporized fraction as obtained in step (a) to obtain a cyclic ester-containing condensate; (c) subjecting at least part of the cyclic ester-containing condensate as obtained in step (b) to melt crystallization to obtain a purified cyclic ester-containing stream and a residue stream; and (d) recovering the purified cyclic ester-containing stream as obtained in step (c). The invention further relates to an apparatus suitable for carrying out the present process.


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