The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 24, 2018

Filed:

Jun. 17, 2014
Applicant:

Wacker Chemie Ag, Munich, DE;

Inventors:

Thorsten Goebel, Emmerting, DE;

Walter Haeckl, Zeilarn, DE;

Wolfgang Muenzer, Kirchdorf, DE;

Uwe Paetzold, Burghausen, DE;

Natalia Sofina, Burghausen, DE;

Assignee:

WACKER CHEMIE AG, Munich, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G01N 21/65 (2006.01); C01B 33/107 (2006.01); G01N 21/3504 (2014.01); G01N 30/14 (2006.01); G01N 30/86 (2006.01); B01D 53/68 (2006.01);
U.S. Cl.
CPC ...
G01N 21/65 (2013.01); B01D 53/685 (2013.01); C01B 33/10742 (2013.01); C01B 33/10763 (2013.01); G01N 21/3504 (2013.01); G01N 30/14 (2013.01); G01N 30/86 (2013.01); B01D 2251/304 (2013.01); B01D 2251/60 (2013.01); B01D 2253/112 (2013.01); B01D 2257/204 (2013.01); B01D 2257/2045 (2013.01); B01D 2258/02 (2013.01); G01N 2201/06113 (2013.01); G01N 2201/08 (2013.01);
Abstract

The composition of a gas or gas stream containing AlClin a chemical reactor is measured by removing AlClfrom the gas and analyzing the gas by gas chromatography or spectroscopy. Chlorosilanes may be prepared in a fluidized bed reactor having a reactor height H0, in which supplied HCl reacts with silicon, wherein a temperature profile in the fluidized bed reactor is greater than S1(H/H0)=(a1−b1)*(1/(1+exp(−c1((H/H0)−d1))))+b1 and less than S2(H/H0)=(a2−b2)*(1/(1+exp(−c2((H/H0)−d2))))+b2, where a1=100° C., a2=300° C., b1=300° C., b2=400° C., c1=50, c2=20, d1=0.2, and d2=0.8.


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