Bayer Aktiengesellschaft

Symrise Ag

Haarmann & Reimer Gmbh

Reinhard Boeck

Heiko Herold

Hans Uhlemann

Jurgen Hinderer

Hans Daun

Birgit Schleifenbaum

Jens Uhlemann

Helmut Mothes

This invention relates to encapsulated flavor and/or fragrance preparations and a method for producing same from a spray solution consisting of an aqueous solution of polymeric carriers and emulsified flavors and/or fragrances. The granules have an adjustable particle size of between 0.2 and 2 mm, present even size distribution and a globular shape and are further characterized by a high concentration and high retention of volatile flavors.

Encapsulated flavor and/or fragrance preparations

By fluidized-bed spray granulation, dextrin granules having a high content of enclosed alcohol are obtained from dextrin/water/alcohol mixtures.

Alcohol-containing granules

Granule production is based on particle growth in a fluidized bed (4), in which the liquid starting product is sprayed into the fluidized bed and the finished granular particle is discharged from the fluidized bed (4) with classification. The classification is carried out with the aid of a classifying air flow which is divided into individual single flows (6) to each of which is assigned a zigzag classifier module (7, 17) and a spray nozzle (5) or a group of spray nozzles. The course of the classifying process is such that the granular particles which are too small and have not yet reached the desired diameter are thrown back into the fluidized bed (4) by a return shaft (9, 18) seated on each of the zigzag classifier modules (7, 17) in parallel or radial zones without cross-mixing, in which the relatively small particles impinge at a relatively large distance from the return shaft (9, 18) and the large particles, which have already grown close to the discharge size, impinge at a relatively small distance. The process is carried out with the aid of a fluidized bed granulator, to the inlet plate (2) of which is connected a zigzag classifier, subdivided in a modular manner, in which each zigzag classifier module (7, 17) is provided with a return shaft (9, 18) at the point where it joins the inlet plate (2, 16). In addition, at least one spray nozzle (5) at the inlet plate (2, 16) is allocated to each zigzag classifier module (7, 17).

Process and device for fluidized bed spray granulation

The zigzag classifier has a classifying space provided with air inlets which is subdivided into zigzag-shaped ducts, which are connected in parallel with respect to the flow, the lengths of which are greater than their widths. In this way a classifier package is formed with a plurality of small duct cross-sections. This design principle permits substantially lower overall heights for the same number of bends.

Growing community of inventors

Kaarst, Germany

Reinhard Boeck