Battelle Memorial Institute

Battelle Development Corporation

Jean-Michel Armanet

Jean-Pierre Sachetto

Herve Tournier

Alain Regnault

Thomas Hamm

Claude Giddey

Alain Roman

Sergio Cuccolo

Gunter Bellmann

Van T Nguyen

Jean-Pierre Michel

Allan A Johansson

Dehydrated protein materials are treated with gaseous HCl without temperature control, the reaction temperature being susceptible to reach, momentarily, 150.degree. C. Then the material thus treated is degassed and, after drying, a non hygroscopic powder usable in the food industry or in the pharmaceutical industry is obtained.

Method for hydrolyzing protein materials

A method for delignifying ligno-cellulosic materials and efficiently separate from each other the constituents thereof. Said materials are heated in an aqueous acid medium in the presence of phenol compounds. Then the reaction medium is drained and washed for isolating the purified solid cellulose pulp, the liquid phase separating into two layers: an aqueous layer rich with pentoses and an organic layer rich with phenols and lignin, the latter providing, by distillation and pyrolysis of the residue, a quantity of phenols at least equal to that of the phenols used in the delignification stage.

Method for the simultaneous delignification of wood and other

Mineral charge particles of silica or alumina are grafted with a hydrolysis product from a di- or trialkoxysilane whose functional group is compatible with an organic phase into which said grafted particles are ultimately incorporated. The grafted particles are separated from the aqueous hydrolysis medium by spray-drying. The organic phase comprising the grafted mineral particles is used to provide coatings with abrasion resistant properties.

Method for manufacturing a composition for coating substrates with an

Continuous hydrolysis to produce sugars is effected by cyclically immersing a solid, divided lignocellulosic material in a bath of concentrated hydrochloric acid and draining the material between successive immersions so as to dissolve the produced sugars, until the sugar concentration of the acid in the bath has attained a desired value. The solid material and the liquid acid are delivered to a tubular horizontal rotary reactor arranged to provide a bath of the acid, to produce a rotating movement for cyclical immersion of the solid material in the bath of acid and longitudinally displace the solid material undergoing hydrolysis together with the acid of the bath and to continuously discharge solid residue and acid containing dissolved sugars due to overflow by gravity at an outlet end of the reactor.

Process and apparatus for continuous acid hydrolysis and saccharification

A fragmented material is dissolved continuously by impregnation and immersion into a solvent bath in which said material is subjected to a moderate mixing movement allowing it to be kept within the interior of said bath to undergo dissolution therein until formation of fine residual particles of insoluble material which are maintained in suspension by this movement, the whole being removed continuously by a controlled overflow of the bath. This process is applied to cellulose contained in various lignocellulosic materials, which is dissolved continuously by immersion of the previously impregnated material into a bath of hydrochloric acid through which hydrogen chloride gas is caused to bubble, to effect complete dissolution of the cellulose and suspension of the fine insoluble residual lignin particles.

Process for continuously dissolving a particulate solid material,

A process for the preparation of lactosylurea and the N-methylol derivative thereof which are usable as feed supplements for ruminants. According to this process, lactose and urea are heated to 70.degree.-110.degree. C. with a minimum of water and, if possible, this water is eliminated during the reaction. The crude reaction product can be purified by grinding with ice-water or ethanol and subsequent draining so as to eliminate by dissolution in such solvants the unreacted urea. The corresponding N-methylol derivative is obtained by the reaction with formaldehyde.

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Onex, Switzerland

Jean-Michel Armanet