The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 05, 2018

Filed:

Mar. 29, 2017
Applicant:

The United States of America As Represented BY the Administrator of the National Aeronautics and Space Administration, Washington, DC (US);

Inventors:

Terry D. Rolin, Elkmont, AL (US);

Ian K. Small, Huntsville, AL (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B05D 3/02 (2006.01); C04B 35/468 (2006.01); C04B 35/626 (2006.01); C04B 35/63 (2006.01); C04B 35/622 (2006.01); C04B 35/64 (2006.01); G01N 27/22 (2006.01); B05D 3/04 (2006.01);
U.S. Cl.
CPC ...
B05D 3/0254 (2013.01); B05D 3/048 (2013.01); B05D 3/0413 (2013.01); B05D 3/0493 (2013.01); C04B 35/4682 (2013.01); C04B 35/6262 (2013.01); C04B 35/6264 (2013.01); C04B 35/62222 (2013.01); C04B 35/6303 (2013.01); C04B 35/64 (2013.01); G01N 27/223 (2013.01); G01N 27/226 (2013.01); C04B 2235/3215 (2013.01); C04B 2235/3227 (2013.01); C04B 2235/3236 (2013.01); C04B 2235/36 (2013.01); C04B 2235/5436 (2013.01); C04B 2235/656 (2013.01); C04B 2235/6581 (2013.01);
Abstract

A method is provided for manufacturing a humidity sensing material. Particles of a trivalent rare earth hydroxide or oxide (such as lanthanum hydroxide) are mixed with particles of barium oxide and titanium dioxide in specified proportions. The particle mixture is heated to generate a sintered mixture that is milled. The resulting milled particles are mixed with glass particles, an organic surfactant, a solvent, an organic vehicle, and an alkali hydroxide. The resulting liquid mixture is deposited as a layer thereof onto a substrate. The substrate and layer thereon are processed to remove liquid portions of the liquid mixture. Such liquid removal processing includes at least one cycle of heating the layer followed by a corresponding cycle of cooling the layer in a nitrogen atmosphere containing less than 25 parts per million of oxygen.


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