The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 29, 2018

Filed:

Sep. 23, 2016
Applicant:

Louisiana Tech Research Corporation, Ruston, LA (US);

Inventors:

David Mills, Monroe, LA (US);

Christen Boyer, Lafayette, LA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B82Y 30/00 (2011.01); A61L 31/12 (2006.01); A61L 31/04 (2006.01); A61L 31/08 (2006.01); A61L 31/16 (2006.01); C09C 1/42 (2006.01); C09C 3/06 (2006.01); C25D 3/46 (2006.01); C25D 3/48 (2006.01); C25D 3/50 (2006.01); C25D 3/38 (2006.01);
U.S. Cl.
CPC ...
A61L 31/128 (2013.01); A61L 31/04 (2013.01); A61L 31/088 (2013.01); A61L 31/16 (2013.01); B82Y 30/00 (2013.01); C09C 1/42 (2013.01); C09C 3/066 (2013.01); C25D 3/38 (2013.01); C25D 3/46 (2013.01); C25D 3/48 (2013.01); C25D 3/50 (2013.01); A61L 2300/102 (2013.01); A61L 2300/104 (2013.01); A61L 2300/404 (2013.01); A61L 2300/606 (2013.01); A61L 2400/12 (2013.01); C01P 2004/13 (2013.01); C01P 2004/80 (2013.01);
Abstract

A method for forming metal nanoparticles on halloysite nanotubes. The method provides a water-based suspension solution containing about 0.002% to about 0.1% by weight of halloysite nanotubes. The suspension solution is maintained between about 2° C. and about 98° C. and under sufficient mixing that the nanotubes are maintained in substantially constant suspension. At least one positive and at least one negative metal electrode is positioned in the suspension solution, wherein the metal electrodes are at least 98% pure metal. A voltage is maintained across the electrodes of between about 10 and about 300 volts for a time sufficient to form metal ions on at least about 10% of a surface of the halloysite nanotubes.


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