The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 01, 2018

Filed:

Feb. 06, 2017
Applicants:

Xin Jack Zhou, Hockessin, DE (US);

Sean Xiaolu Wang, Wilmington, DE (US);

Qun LI, Newark, DE (US);

Inventors:

Xin Jack Zhou, Hockessin, DE (US);

Sean Xiaolu Wang, Wilmington, DE (US);

Qun Li, Newark, DE (US);

Assignee:

BWT Property, Inc., Newark, DE (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G01N 21/71 (2006.01); G01N 33/20 (2006.01); H01S 5/06 (2006.01); G01J 3/443 (2006.01);
U.S. Cl.
CPC ...
G01N 21/718 (2013.01); G01J 3/443 (2013.01); G01N 33/20 (2013.01); H01S 5/0615 (2013.01);
Abstract

This invention discloses an improved laser induced breakdown spectroscopy (LIBS) apparatus and method for the detection of mineral and metal contamination in liquid samples. The mineral and metal contaminant is first collected by filtering the liquid sample with a membrane filter. The membrane filter with the mineral and metal contaminant is then measured by a LIBS apparatus. The LIBS apparatus is based on a high repetition rate pulsed laser. The laser produces a train of laser pulses at a high repetition rate in the kHz (or even higher) range. When the laser beam hits the surface of the membrane filter, it generates several thousands of micro-plasma emissions per second. Synchronized miniature CCD array optical spectrometer modules collect the LIBS signal from these micro-plasma emissions. By adjusting the integration time of the spectrometer to cover a plurality of periods of the laser pulse train, the spectrometer integrates the LIBS signal produced by this plurality of laser pulses. Hence the intensity of the obtained LIBS spectrum can be greatly improved to increase the signal-to-noise ratio (SNR) and lower the level of detection (LOD).


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