The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 01, 2018

Filed:

Nov. 10, 2016
Applicant:

Celanese International Corporation, Irving, TX (US);

Inventors:

Ronald D. Shaver, Houston, TX (US);

Yaw-Hwa Liu, Missouri City, TX (US);

Mark O. Scates, Houston, TX (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/12 (2006.01); C07C 51/44 (2006.01); C07C 51/47 (2006.01);
U.S. Cl.
CPC ...
C07C 51/12 (2013.01); C07C 51/44 (2013.01); C07C 51/445 (2013.01); C07C 51/47 (2013.01);
Abstract

Process for producing acetic acid are disclosed in which a vapor sidedraw is withdrawn from the second column in the primary purification train. The vapor sidedraw comprises acetic acid and lithium-containing compounds at a concentration of no more than 100 wppb. A bottoms stream that is enriched in lithium-containing compounds, such as lithium acetate, or lithium acetate dihydrate, is also withdrawn from the second column. Advantageously, the vapor sidedraw, or a condensed portion thereof, is directly fed to a metal-exchanged ion exchange resin having acid cation exchange sites to produce purified acetic acid. This prevents displacement of the metals in the ion exchange resin.


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