The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 01, 2018

Filed:

Apr. 25, 2014
Applicant:

Basf SE, Ludwigshafen, DE;

Inventors:

Friedrich-Georg Martin, Heidelberg, DE;

Oliver Odenwald, Dielheim, DE;

Assignee:

BASF SE, Ludwigshafen, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07B 63/04 (2006.01); B01J 19/00 (2006.01); B01J 4/00 (2006.01);
U.S. Cl.
CPC ...
C07B 63/04 (2013.01); B01J 4/001 (2013.01); B01J 19/002 (2013.01); B01J 2219/00272 (2013.01);
Abstract

The present invention relates to a process for restabilizing free-radically polymerizable monomers. The process comprises the steps: (a) introduction of a solution of an inhibitor of the free-radical polymerization by means of an inert pressurized gas into a vessel () comprising the monomers via a line () which comprises an ascending region, and (b) mixing of the contents of the vessel and the inhibitor solution by blowing gas through the line (). In step (a), the flow velocity of the pressurized gas is set so that plug flow or annular flow is obtained as flow regime of the inhibitor solution and in step (b) the superficial gas velocity is set to ≥0.1 mm/s. The present invention further relates to a supply unit () for carrying out the process.


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