The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 27, 2018

Filed:

Mar. 22, 2016
Applicant:

The United States of America As Represented BY the Secretary of the Air Force, Washington, DC (US);

Inventors:

James M Mann, Springboro, OH (US);

Joseph Kolis, Central, SC (US);

Eric Hunt, Glen Rock, PA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C30B 29/10 (2006.01); C30B 7/10 (2006.01); C01B 25/45 (2006.01); C09K 11/77 (2006.01); C30B 29/14 (2006.01); C01G 43/025 (2006.01); C30B 7/14 (2006.01); C30B 29/16 (2006.01); C01G 43/00 (2006.01); C01G 43/06 (2006.01); C30B 29/12 (2006.01); C01B 25/455 (2006.01); C09K 11/04 (2006.01);
U.S. Cl.
CPC ...
C30B 7/10 (2013.01); C01B 25/45 (2013.01); C01B 25/455 (2013.01); C01G 43/006 (2013.01); C01G 43/025 (2013.01); C01G 43/06 (2013.01); C09K 11/04 (2013.01); C09K 11/7709 (2013.01); C30B 7/14 (2013.01); C30B 29/12 (2013.01); C30B 29/14 (2013.01); C30B 29/16 (2013.01); C01P 2002/72 (2013.01); C01P 2002/76 (2013.01); C01P 2002/77 (2013.01); C01P 2006/60 (2013.01);
Abstract

A method of synthesizing uranium dioxide crystals. The method of synthesizing includes combining a uranium-based feedstock with a mineralizer solution. The uranium-based feedstock is selected from uranium dioxide, uranium tetrafluoride, uranium tetrachloride, triuranium octoxide, and uranium trioxide. The feedstock and mineralizer solution are pressurized, and then a thermal gradient is applied thereto such that a first portion of the feedstock and the mineralizer solution is heated to a temperature that is greater than a temperature of a second portion of the feedstock and the mineralizer solution. The uranium nutrient enters the mineralizer solution from the feedstock in the first portion and uranium nutrient precipitates to spontaneously form crystals in the second portion.


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