The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 13, 2018

Filed:

Nov. 17, 2016
Applicants:

Aruna Zhamu, Springboro, OH (US);

Wei Xiong, Kettering, OH (US);

Bor Z. Jang, Centerville, OH (US);

Inventors:

Aruna Zhamu, Springboro, OH (US);

Wei Xiong, Kettering, OH (US);

Bor Z. Jang, Centerville, OH (US);

Assignee:

Nanotek Instruments, Inc., Dayton, OH (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C30B 1/02 (2006.01); C30B 29/02 (2006.01); C30B 5/00 (2006.01); C30B 29/68 (2006.01); C01B 32/22 (2017.01); C01B 32/225 (2017.01); C01B 32/23 (2017.01); C01B 32/182 (2017.01); C01B 32/184 (2017.01); C01B 32/19 (2017.01); C01B 32/192 (2017.01); B82Y 30/00 (2011.01); B82Y 40/00 (2011.01);
U.S. Cl.
CPC ...
C30B 1/02 (2013.01); C01B 32/182 (2017.08); C01B 32/184 (2017.08); C01B 32/19 (2017.08); C01B 32/192 (2017.08); C01B 32/22 (2017.08); C01B 32/225 (2017.08); C01B 32/23 (2017.08); C30B 5/00 (2013.01); C30B 29/02 (2013.01); C30B 29/68 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01); C01P 2006/10 (2013.01); C01P 2006/32 (2013.01); C01P 2006/40 (2013.01); C01P 2006/80 (2013.01); Y10S 977/734 (2013.01); Y10S 977/842 (2013.01); Y10T 428/30 (2015.01);
Abstract

A unitary graphene layer or graphene single crystal containing closely packed and chemically bonded parallel graphene planes having an inter-graphene plane spacing of 0.335 to 0.40 nm and an oxygen content of 0.01% to 10% by weight, which unitary graphene layer or graphene single crystal is obtained from heat-treating a graphene oxide gel at a temperature higher than 100° C., wherein the average mis-orientation angle between two graphene planes is less than 10 degrees, more typically less than 5 degrees. The molecules in the graphene oxide gel, upon drying and heat-treating, are chemically interconnected and integrated into a unitary graphene entity containing no discrete graphite flake or graphene platelet. This graphene monolith exhibits a combination of exceptional thermal conductivity, electrical conductivity, mechanical strength, surface smoothness, surface hardness, and scratch resistance unmatched by any thin-film material of comparable thickness range.


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