The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 13, 2018

Filed:

Dec. 28, 2011
Applicants:

Charles Schenck Wiley, Charlotte, NC (US);

Robert F. Speyer, Atlanta, GA (US);

Inventors:

Charles Schenck Wiley, Charlotte, NC (US);

Robert F. Speyer, Atlanta, GA (US);

Assignee:

VERCO MATERIALS, LLC, Atlanta, GA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C04B 35/563 (2006.01); C04B 35/626 (2006.01); C04B 35/628 (2006.01); C04B 35/632 (2006.01); C04B 35/634 (2006.01); C04B 35/645 (2006.01); C04B 33/32 (2006.01);
U.S. Cl.
CPC ...
C04B 35/563 (2013.01); C04B 33/32 (2013.01); C04B 35/62655 (2013.01); C04B 35/62695 (2013.01); C04B 35/62821 (2013.01); C04B 35/6325 (2013.01); C04B 35/63476 (2013.01); C04B 35/6455 (2013.01); C04B 2235/3813 (2013.01); C04B 2235/3821 (2013.01); C04B 2235/3826 (2013.01); C04B 2235/422 (2013.01); C04B 2235/425 (2013.01); C04B 2235/449 (2013.01); C04B 2235/48 (2013.01); C04B 2235/5409 (2013.01); C04B 2235/5445 (2013.01); C04B 2235/5481 (2013.01); C04B 2235/656 (2013.01); C04B 2235/6562 (2013.01); C04B 2235/6565 (2013.01); C04B 2235/661 (2013.01); C04B 2235/668 (2013.01); C04B 2235/77 (2013.01); C04B 2235/784 (2013.01); C04B 2235/785 (2013.01); C04B 2235/786 (2013.01); C04B 2235/80 (2013.01); C04B 2235/96 (2013.01);
Abstract

Disclosed is a method for fabricating a solid article from a boron carbide powder comprising boron carbide particles that are coated with a titanium compound. Further disclosed herein are the unique advantages of the combined use of titanium and graphite additives in the form of water soluble species to improve intimacy of mixing in the green state. The carbon facilitates sintering, whose concentration is then attenuated in the process of forming very hard, finely dispersed Ti B2 phases. The further recognition of the merits of a narrow particle size distribution B4C powder and the use of sintering soak temperatures at the threshold of close porosity which achieve post-HIPed microstructures with average grain sizes approaching the original median particle size. The combination of interdependent factors has led to B4C-based articles of higher hardness than previously reported.


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