The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 06, 2018

Filed:

May. 24, 2016
Applicant:

Ut-battelle, Llc, Oak Ridge, TN (US);

Inventors:

Zachary D. Hood, Atlanta, GA (US);

Shiba P. Adhikari, Winston Salem, NC (US);

Marcus W. Wright, King, NC (US);

Abdessadek Lachgar, Winston Salem, NC (US);

Yunchao Li, Knoxville, TN (US);

Amit K. Naskar, Knoxville, TN (US);

Mariappan Parans Paranthaman, Knoxville, TN (US);

Assignees:

UT-BATTELLE, LLC, Oak Ridge, TN (US);

UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION, Knoxville, TN (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/08 (2006.01); C01B 31/08 (2006.01); B01J 31/02 (2006.01); B01J 35/02 (2006.01); B01J 35/10 (2006.01); B01J 37/08 (2006.01); B01J 37/00 (2006.01);
U.S. Cl.
CPC ...
C07C 67/08 (2013.01); B01J 31/0225 (2013.01); B01J 35/026 (2013.01); B01J 35/1057 (2013.01); B01J 35/1061 (2013.01); B01J 37/0072 (2013.01); B01J 37/084 (2013.01); C01B 31/081 (2013.01); B01J 2231/49 (2013.01); B01J 2531/004 (2013.01);
Abstract

A method of making solid acid catalysts includes the step of sulfonating waste tire pieces in a first sulfonation step. The sulfonated waste tire pieces are pyrolyzed to produce carbon composite pieces having a pore size less than 10 nm. The carbon composite pieces are then ground to produce carbon composite powders having a size less than 50 μm. The carbon composite particles are sulfonated in a second sulfonation step to produce sulfonated solid acid catalysts. A method of making biofuels and solid acid catalysts are also disclosed.


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