The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 12, 2017

Filed:

Sep. 15, 2015
Applicant:

Expression Pathology, Inc., Rockville, MD (US);

Inventors:

David B. Krizman, Gaithersburg, MD (US);

Todd Hembrough, Gaithersburg, MD (US);

Sheeno Thyparambil, Frederick, MD (US);

Wei-Li Liao, Herndon, VA (US);

Assignee:

Expression Pathology, Inc., Rockville, MD (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
A61K 38/10 (2006.01); A61K 38/00 (2006.01); C12Q 1/37 (2006.01); G01N 33/574 (2006.01); G01N 33/68 (2006.01); C07K 16/40 (2006.01); C12N 9/10 (2006.01); C12N 9/12 (2006.01);
U.S. Cl.
CPC ...
C12Q 1/37 (2013.01); C07K 16/40 (2013.01); C12N 9/1007 (2013.01); C12N 9/12 (2013.01); G01N 33/57484 (2013.01); G01N 33/6848 (2013.01); C07K 2317/34 (2013.01); C12Y 201/01045 (2013.01); C12Y 207/10001 (2013.01); G01N 2560/00 (2013.01); G01N 2800/52 (2013.01); G01N 2800/56 (2013.01); G01N 2800/7028 (2013.01);
Abstract

The current disclosure provides for specific peptides, and derived ionization characteristics of the peptides, from the ALK, Ros, Ron, Ret, TS, and/or FGFR1 proteins that are particularly advantageous for quantifying the ALK, Ros, Ron, Ret, TS, and/or FGFR1 proteins directly in biological samples that have been fixed in formalin by the methods of Selected Reaction Monitoring (SRM) mass spectrometry, or as Multiple Reaction Monitoring (MRM) mass spectrometry. Such biological samples are chemically preserved and fixed wherein the biological sample is selected from tissues and cells treated with formaldehyde containing agents/fixatives including formalin-fixed tissue/cells, formalin-fixed/paraffin embedded (FFPE) tissue/cells, FFPE tissue blocks and cells from those blocks, and tissue culture cells that have been formalin fixed and or paraffin embedded. A protein sample is prepared from the biological sample using the Liquid Tissue™ reagents and protocol and the ALK, Ros, Ron, Ret, TS, and/or FGFR1 proteins are quantitated in the Liquid Tissue™ sample by the method of SRM/MRM mass spectrometry, by quantitating in the protein sample at least one or more of the peptides described. These peptides can be quantitated if they reside in a modified or an unmodified form. An example of a modified form of an ALK, Ros, Ron, Ret, TS, and/or FGFR1 fragment peptide is phosphorylation of a tyrosine, threonine, serine, and/or other amino acid residues within the peptide sequence.


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