The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 21, 2017

Filed:

Dec. 14, 2016
Applicant:

Shell Oil Company, Houston, TX (US);

Inventors:

Andries Quirin Maria Boon, Houston, TX (US);

Joseph Broun Powell, Houston, TX (US);

Assignee:

SHELL OIL COMPANY, Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/00 (2006.01); B01J 37/00 (2006.01); C10G 3/00 (2006.01); C07C 29/145 (2006.01); B01J 37/20 (2006.01); C10G 1/06 (2006.01); B01J 23/755 (2006.01); B01J 23/882 (2006.01);
U.S. Cl.
CPC ...
C07C 29/145 (2013.01); B01J 37/20 (2013.01); C10G 1/065 (2013.01); C10G 3/00 (2013.01); B01J 23/755 (2013.01); B01J 23/882 (2013.01);
Abstract

A method of extending the catalyst life of a hydrogenolysis catalyst activity in the presence of biomass and aqueous solution is described. Lignocellulosic biomass solids and aqueous solution is provided to in a hydrothermal digestion unit in the presence of a digestive solvent, and a supported hydrogenolysis catalyst containing (a) sulfur, (b) Mo or W, and (c) Co, Ni or mixture thereof, incorporated into a solid metal oxide support. The lignocellulosic biomass solids in the hydrothermal digestion unit is heated to a temperature in the range of 180° C. to less than 300° C. in the presence of digestive solvent, hydrogen, and in the range of 0.15 wt. % to 12.5 wt. %, based on catalyst, of HS or HS source at least partially soluble in aqueous solution, and the supported hydrogenolysis catalyst forming a product solution containing plurality of oxygenated hydrocarbons, the hydrothermal digestion unit maintaining protective sulfur concentration.


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