The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 17, 2017

Filed:

Jun. 27, 2014
Applicant:

Yale University, New Haven, CT (US);

Inventors:

Stafford Wheeler Sheehan, Tiverton, RI (US);

Ulrich Hintermair, Rottendorf, DE;

Julianne M. Thomsen, Colton, CA (US);

Gary W. Brudvig, Orange, CT (US);

Robert H. Crabtree, Bethany, CT (US);

Assignee:

Yale University, New Haven, CT (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C25B 11/04 (2006.01); C02F 1/467 (2006.01); H01M 4/92 (2006.01); C25B 1/00 (2006.01); C25B 3/02 (2006.01); C07C 309/44 (2006.01); C07C 303/32 (2006.01); C07F 15/00 (2006.01); C07F 17/00 (2006.01); C02F 1/461 (2006.01);
U.S. Cl.
CPC ...
C25B 11/0489 (2013.01); C02F 1/4672 (2013.01); C07C 303/32 (2013.01); C07C 309/44 (2013.01); C07F 15/0033 (2013.01); C07F 17/00 (2013.01); C25B 1/003 (2013.01); C25B 3/02 (2013.01); C25B 11/0405 (2013.01); C25B 11/0447 (2013.01); H01M 4/923 (2013.01); H01M 4/926 (2013.01); C02F 2001/46142 (2013.01); C02F 2303/10 (2013.01); H01M 4/925 (2013.01); Y02W 10/30 (2015.05);
Abstract

Solution-phase (e.g., homogeneous) or surface-immobilized (e.g., heterogeneous) electrode-driven oxidation catalysts based on iridium coordination compounds which self-assemble upon chemical or electrochemical oxidation of suitable precursors and methods of making and using thereof are. Iridium species such as {[Ir(LX)(HO)(μ-O)]}wherein x, y, m are integers from 0-4, z and n from 1-4 and LX is an oxidation-resistant chelate ligand or ligands, such as such as 2(2-pyridyl)-2-propanolate, form upon oxidation of various molecular iridium complexes, for instance [Cp*Ir(LX)OH] or [(cod)Ir(LX)] (Cp*=pentamethylcyclopentadienyl, cod=cis-cis,1,5-cyclooctadiene) when exposed to oxidative conditions, such as sodium periodate (NaIO) in aqueous solution at ambient conditions.


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