The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 10, 2017

Filed:

Mar. 23, 2015
Applicant:

Wacker Chemie Ag, Munich, DE;

Inventor:

Peter Gigler, Dachau, DE;

Assignee:

Wacker Chemie AG, Munich, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 23/46 (2006.01); C07C 67/343 (2006.01); B01J 35/12 (2006.01); B01J 37/16 (2006.01);
U.S. Cl.
CPC ...
B01J 23/462 (2013.01); B01J 35/12 (2013.01); B01J 37/16 (2013.01); C07C 67/343 (2013.01);
Abstract

The invention relates to a method for providing a ruthenium catalyst solution which is active during the transvinylation of a surfactant vinyl ester with a surfactant carboxylic acid, comprising an Ru metal concentration of more than 0.5 wt. % based on the total weight of the ruthenium catalyst solution. The invention is characterized in that a) at least one ruthenium (III) halogenide with at least one inorganic or organic base, at least one surfactant vinyl ester, and at least one surfactant carboxylic acid is reacted at a temperature of 70° C. to 170° C.; b) the molar ratio of surfactant vinyl ester to surfactant carboxylic acid is 1:1.8 to 1.8:1; and c) the ruthenium (III) halogenide is used in a quantity of >0.5 wt. % of Ru metal based on the total weight of the surfactant vinyl ester and surfactant carboxylic acid.


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