The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 10, 2017

Filed:

Dec. 07, 2011
Applicants:

Hiroki Mikuni, Hitachi, JP;

Kiyoshi Kawai, Hitachinaka, JP;

Inventors:

Hiroki Mikuni, Hitachi, JP;

Kiyoshi Kawai, Hitachinaka, JP;

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01J 20/28 (2006.01); C01B 33/26 (2006.01); C02F 1/28 (2006.01); B01J 20/10 (2006.01); B01J 20/30 (2006.01); B01J 20/16 (2006.01); C02F 101/20 (2006.01);
U.S. Cl.
CPC ...
B01J 20/2808 (2013.01); B01J 20/10 (2013.01); B01J 20/16 (2013.01); B01J 20/28061 (2013.01); B01J 20/28069 (2013.01); B01J 20/28078 (2013.01); B01J 20/3085 (2013.01); C01B 33/26 (2013.01); C02F 1/281 (2013.01); C01P 2002/72 (2013.01); C01P 2006/12 (2013.01); C01P 2006/14 (2013.01); C01P 2006/16 (2013.01); C02F 2101/20 (2013.01);
Abstract

The aluminum silicate of the invention has: an element ratio of Si and Al, represented by Si/Al, of from 0.3 to 1.0 by molar ratio; a peak at approximately 3 ppm in aAl-NMR spectrum; peak A at approximately −78 ppm and peak B at approximately −85 ppm in aSi-NMR spectrum; and a peak at approximately 2θ=26.9° and a peak at approximately 2θ=40.3° in a powder X-ray diffraction spectrum. The aluminum silicate has an area ratio of peak B with respect to peak A of from 2.0 to 9.0, or does not include a tubular substance having a length of 50 nm or more as observed in a transmission electron microscope (TEM) photograph of the aluminum silicate taken at a magnification of 100,000. The aluminum silicate is produced by a method comprising: subjecting a reaction product of a silicate ion solution and an aluminum ion solution to desalting and solid separation; subjecting a resultant to a thermal treatment in an aqueous medium in the presence of an acid under concentration conditions in an aqueous medium such that a silicon atom concentration is 100 mmol/L or more and an aluminum atom concentration is 100 mmol/L or more; and subjecting a resultant to further desalting and solid separation.


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