The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 19, 2017

Filed:

Apr. 09, 2009
Applicants:

Charles Guthrie Moyers, Charleston, WV (US);

James Kermit Withrow, Charleston, WV (US);

John Leonard Stephens, Hurricane, WV (US);

Inventors:

Charles Guthrie Moyers, Charleston, WV (US);

James Kermit Withrow, Charleston, WV (US);

John Leonard Stephens, Hurricane, WV (US);

Assignee:

Iowa Corn Promotion Board, Johnston, IA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
A61K 31/495 (2006.01); A61K 31/7048 (2006.01); A61K 9/28 (2006.01); A61K 9/48 (2006.01); C07D 493/04 (2006.01); C07H 1/06 (2006.01);
U.S. Cl.
CPC ...
C07D 493/04 (2013.01); C07H 1/06 (2013.01);
Abstract

A process for the production of a refined dianhydrosugar-containing product is disclosed. The process includes controlled continuous crystallization of the dianhydrosugar-containing product to produce a solution saturated with the dianhydrosugar. The saturated solution is mechanically separated, for example by centrifugation, and the crystalline product is washed. The only solvent used is water. The dianhydrosugar-containing product is upgraded to at least 99.8% purity and recovery is 95% or greater. Recrystallization of the dianhydrosugar of 99.8% purity results in an ultra pure product containing at least 99.99% dianhydrosugar.


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