The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 12, 2017

Filed:

May. 02, 2014
Applicants:

Dow Global Technologies Llc, Midland, MI (US);

Rohm and Haas Company, Philadelphia, PA (US);

Inventors:

Ronda L. Gras, Edmonton, CA;

Jim C. Luong, Sherwood Park, CA;

Warren E. Smith, Buckinghamshire, GB;

Assignees:

ROHM AND HAAS COMPANY, Philadelphia, PA (US);

DOW GLOBAL TECHNOLOGIES LLC, Midland, MI (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N 30/72 (2006.01); G01N 33/28 (2006.01); C10L 1/00 (2006.01); G01N 30/46 (2006.01); G01N 30/60 (2006.01); G01N 30/88 (2006.01); G01N 30/04 (2006.01);
U.S. Cl.
CPC ...
G01N 30/7206 (2013.01); C10L 1/003 (2013.01); G01N 30/463 (2013.01); G01N 30/6078 (2013.01); G01N 30/88 (2013.01); G01N 33/28 (2013.01); G01N 33/2882 (2013.01); G01N 30/465 (2013.01); G01N 30/7233 (2013.01); G01N 2030/042 (2013.01); G01N 2030/8854 (2013.01);
Abstract

A gas chromatographic method for detecting a marker compound in a fuel by (a) introducing a sample of fuel into a first capillary column coated with a stationary phase based on polydimethylsiloxane and allowing the sample to flow through the first column to produce a first effluent; (b) allowing the first effluent to pass through a detector and identifying a retention time range in it which includes a retention time of the marker compound; (c) introducing only a portion of the first effluent stream which is within the retention time range into a second capillary column coated with either (i) an ionic sorbent or (ii) a polyethylene glycol, and allowing said portion to flow through the second capillary column to produce a second effluent stream; and (d) allowing the second effluent to pass through a detector; wherein the marker compound has formula Ar(R)(OR)and is present in the fuel at a level from 0.01 ppm to 100 ppm.


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