The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 05, 2017

Filed:

Jun. 28, 2013
Applicant:

The Provost, Fellows, Foundation Scholars & the Other Members of Board, of the College of the Holy & Undiv. Trinity of Queen Elizabeth Near Dublin, College Green, Dublin, IE;

Inventors:

Jonathan Coleman, Dublin, IE;

Umar Khan, Dublin, IE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 13/14 (2006.01); C01B 19/04 (2006.01); C01B 21/083 (2006.01); H01B 1/08 (2006.01); H01B 1/06 (2006.01); H01B 1/10 (2006.01); H01B 3/02 (2006.01); H01B 3/10 (2006.01); C01G 23/04 (2006.01); C01G 25/02 (2006.01); C01G 27/02 (2006.01); C01G 33/00 (2006.01); C01G 35/00 (2006.01); C01G 37/02 (2006.01); C01G 45/02 (2006.01); C01G 41/02 (2006.01); C01G 99/00 (2010.01); C01G 47/00 (2006.01); C01G 53/04 (2006.01); C01G 49/02 (2006.01); C01B 21/064 (2006.01); C01G 31/02 (2006.01); C01G 39/02 (2006.01); C01G 55/00 (2006.01); C01B 19/00 (2006.01); C01G 1/02 (2006.01); C01G 1/12 (2006.01); C01B 31/04 (2006.01); B82Y 30/00 (2011.01); B82Y 40/00 (2011.01);
U.S. Cl.
CPC ...
C01B 13/145 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01); C01B 19/007 (2013.01); C01B 19/04 (2013.01); C01B 21/0648 (2013.01); C01B 21/083 (2013.01); C01B 31/0469 (2013.01); C01G 1/02 (2013.01); C01G 1/12 (2013.01); C01G 23/04 (2013.01); C01G 25/02 (2013.01); C01G 27/02 (2013.01); C01G 31/02 (2013.01); C01G 33/00 (2013.01); C01G 35/00 (2013.01); C01G 37/02 (2013.01); C01G 39/02 (2013.01); C01G 41/02 (2013.01); C01G 45/02 (2013.01); C01G 47/00 (2013.01); C01G 49/02 (2013.01); C01G 53/04 (2013.01); C01G 55/004 (2013.01); C01G 99/00 (2013.01); H01B 1/06 (2013.01); H01B 1/08 (2013.01); H01B 1/10 (2013.01); H01B 3/02 (2013.01); H01B 3/10 (2013.01); C01P 2002/01 (2013.01); C01P 2002/20 (2013.01); C01P 2004/03 (2013.01); C01P 2004/04 (2013.01); C01P 2004/24 (2013.01); Y10T 428/2991 (2015.01);
Abstract

The invention provides a process for exfoliating a 3-dimensional layered material to produce a 2-dimensional material, said process comprising the steps of mixing the layered material in a solvent to provide a mixture; applying energy, for example ultrasound, to said mixture, and removing the energy applied to the mixture, such that sedimentation of the 2-dimensional material out of solution as a weakly re-aggregated, exfoliated 2-dimensional material is produced. The invention provides a fast, simple and high yielding process for separating 3-dimensional layered materials into individual 2-dimensional layers or flakes, which do not strongly re-aggregate, without utilising hazardous solvents.


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