The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 08, 2017

Filed:

Nov. 06, 2012
Applicant:

Technical Institute of Physics and Chemistry of the Chinese Academy of Sciences, Beijing, CN;

Inventors:

Min Wu, Beijing, CN;

Yong Huang, Beijing, CN;

Shigenori Kuga, Beijing, CN;

Pei Huang, Beijing, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08L 1/12 (2006.01); D01F 2/28 (2006.01); C08B 3/00 (2006.01); C08B 3/20 (2006.01); C08B 16/00 (2006.01); C08L 1/10 (2006.01);
U.S. Cl.
CPC ...
C08L 1/12 (2013.01); C08B 3/00 (2013.01); C08B 3/20 (2013.01); C08B 16/00 (2013.01); C08L 1/10 (2013.01); D01F 2/28 (2013.01); C08L 2201/56 (2013.01); C08L 2205/16 (2013.01);
Abstract

A method for preparing stably dispersed cellulose nanofibers comprises the following steps: 1) mixing cellulose and an organic solvent, the percentage of the cellulose being 1% to 15% in weight; 2) adding an esterification agent into the resultant mixture of step 1), the molar ratio of the esterification agent to the cellulose being from 1:0.1 to 4; and 3) physically breaking the resultant mixture of step 2) until a suspension liquid with stably dispersed cellulose nanofibers of 2-1000 nm in diameter and 10-100 μm in length is obtained, an esterification reaction of hydroxyl group(s) on the surface of cellulose fibers occurring at the time of the breaking. Also disclosed are dispersed cellulose nanofibers with improved compatibility to the matrix than the untreated cellulose and an improved strength of the composite materials.


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