The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 08, 2017

Filed:

Jun. 21, 2013
Applicant:

Reg Seneca, Llc, Ames, IA (US);

Inventors:

John P. Jackam, Butte, MT (US);

Derek J. Winkel, Ankeny, IA (US);

Jared A. Downey, Ames, IA (US);

Assignee:

REG Seneca, LLC, Ames, IA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 67/03 (2006.01); C10L 1/02 (2006.01); C11C 3/00 (2006.01); C11C 3/02 (2006.01);
U.S. Cl.
CPC ...
C07C 67/03 (2013.01); C10L 1/026 (2013.01); C11C 3/003 (2013.01); C11C 3/02 (2013.01); C11C 3/025 (2013.01); C10L 2200/0476 (2013.01); Y02E 50/13 (2013.01); Y02P 20/127 (2015.11);
Abstract

A system and method for the conversion of free fatty acids to glycerides and the subsequent conversion of glycerides to glycerin and biodiesel includes the transesterification of a glyceride stream with an alcohol. The fatty acid alkyl esters are separated from the glycerin to produce a first liquid phase containing a fatty acid alkyl ester rich (concentrated) stream and a second liquid phase containing a glycerin rich (concentrated) stream. The fatty acid alkyl ester rich stream is then subjected to distillation, preferably reactive distillation, wherein the stream undergoes both physical separation and chemical reaction. The fatty acid alkyl ester rich stream is then purified to produce a purified biodiesel product and a glyceride rich residue stream. The glycerin rich second liquid phase stream may further be purified to produce a purified glycerin product and a (second) wet alcohol stream. Neutralization of the alkaline stream, formed during the alkali-catalyzed transesterification process, may proceed by the addition of a mineral or an organic acid.


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