The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 01, 2017

Filed:

Mar. 04, 2015
Applicant:

Zhejiang Hisun Pharmaceutical Co., Ltd., Taizhou, CN;

Inventors:

Liang Zhang, Taizhou, CN;

Chuan Liu, Taizhou, CN;

Jinyi Xu, Taizhou, CN;

Zhaozhao Zhang, Taizhou, CN;

Zhi Chen, Taizhou, CN;

Jian Chai, Taizhou, CN;

Zhiqing Yang, Taizhou, CN;

Hairong Luo, Taizhou, CN;

Xiangyang Zhang, Taizhou, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 401/12 (2006.01); C07C 309/04 (2006.01); C07C 303/44 (2006.01); C07D 403/12 (2006.01);
U.S. Cl.
CPC ...
C07D 401/12 (2013.01); C07C 303/44 (2013.01); C07C 309/04 (2013.01); C07D 403/12 (2013.01); C07B 2200/13 (2013.01);
Abstract

The present invention relates to novel crystal forms M and N of dabigatran etexilate mesylate and preparation method and uses thereof, wherein the X-Ray powder diffractogram of the crystal form M has characteristic peaks at the following 2θ diffraction angles: 5.7±0.2°, 6.2±0.2°, 11.2±0.2°, 12.4±0.2°, 18.2±0.2°, 21.4±0.2°, 21.8±0.2° and 23.6±0.2°; and the X-Ray powder diffractogram of the crystal form N has characteristic peaks at the following 2θ diffraction angles: 6.0±0.2°, 11.8±0.2°, 18.2±0.2°, 21.6±0.2°, 24.4±0.2°, 27.7±0.2° and 29.7±0.2°. The crystal forms of the present invention have excellent properties in the aspects of leaching time, biological release, chemical stability and processing adaptability.


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