The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 13, 2017

Filed:

Dec. 08, 2015
Applicant:

Invista North America S.a R.l., Wilmington, DE (US);

Inventors:

William J. Tenn, III, Beaumont, TX (US);

Sudhir N. V. K. Aki, Katy, TX (US);

Thomas E. Vos, Beaumont, TX (US);

Tseng H. Chao, Beaumont, TX (US);

Assignee:

INVISTA NORTH AMERICA S.A.R.L., Wilmington, DE (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B01J 38/56 (2006.01); C07F 9/48 (2006.01); B01J 31/40 (2006.01); B01J 31/18 (2006.01); B01D 11/04 (2006.01); B01D 11/00 (2006.01);
U.S. Cl.
CPC ...
C07F 9/4841 (2013.01); B01D 11/0426 (2013.01); B01D 11/0434 (2013.01); B01D 11/0488 (2013.01); B01D 11/0492 (2013.01); B01J 31/4053 (2013.01); B01J 38/56 (2013.01); B01D 2011/002 (2013.01); B01J 31/1865 (2013.01); B01J 2231/343 (2013.01); B01J 2531/847 (2013.01); Y02P 20/582 (2015.11); Y02P 20/584 (2015.11);
Abstract

Disclosed herein are methods for recovering diphosphonite-containing compounds from mixtures comprising organic mononitriles and organic dinitriles, using multistage countercurrent liquid-liquid extraction. Recovery is enhanced with one or more method steps. In a first step, a portion of the heavy phase from the settling section of the first stage is recycled to the settling section of the first stage. In a second step, a portion of the light phase from the settling section of the first stage is recycled to the mixing section of the first stage. In a third step, the first stage takes place in a mixer-settler, a Lewis base is introduced into the settling section of the first stage, and a complex of Lewis acid and Lewis base is formed in this settling section. In a fourth step, a polyamine is added to the first stage.


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