The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 06, 2017

Filed:

Feb. 11, 2016
Applicant:

Basf SE, Ludwigshafen, DE;

Inventors:

Uwe Storzum, League City, TX (US);

Boris Breitscheidel, Waldsee, DE;

Kevin Scott Todd, Lake Jackson, TX (US);

Jason David Veinot, Cornwall, CA;

Assignee:

BASF SE, Ludwigshafen, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 67/08 (2006.01); C08K 5/12 (2006.01);
U.S. Cl.
CPC ...
C07C 67/08 (2013.01); C08K 5/12 (2013.01);
Abstract

A method for preparing an aromatic di-ester includes combining an aromatic di-acid and a linear or branched C4-C13 alcohol to form a mixture. The method also includes heating the mixture from a first temperature (T1) to a second temperature (T2) without a catalyst present in the mixture. The method further includes combining a titanium catalyst with the mixture after the mixture is at the second temperature (T2). The method further includes increasing pressure from a first pressure (P1) to a second pressure (P2) after the mixture is at the second temperature (T2). The method further includes increasing the temperature of the mixture from the second temperature (T2) to a third temperature (T3) while maintaining the second pressure (P2).


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