The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 9624600 B1

PDF
Full Text
Expired
Date of Patent:
Apr. 18, 2017

Filed:

Dec. 06, 2012
Applicant:

University of North Texas, Denton, TX (US);

Inventor:

Jeffry A. Kelber, Denton, TX (US);

Assignee:

UNIVERSITY OF NORTH TEXAS, Denton, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01L 21/02 (2006.01); H01L 29/82 (2006.01); C30B 23/02 (2006.01); H01L 29/16 (2006.01); H01F 41/32 (2006.01); C30B 29/02 (2006.01); C01B 31/04 (2006.01); B82Y 30/00 (2011.01); B82Y 40/00 (2011.01); C30B 23/06 (2006.01); H01L 29/66 (2006.01);
U.S. Cl.
CPC ...
C30B 23/025 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01); C01B 31/0461 (2013.01); C30B 23/02 (2013.01); C30B 23/066 (2013.01); C30B 29/02 (2013.01); H01F 41/32 (2013.01); H01L 21/02381 (2013.01); H01L 21/02395 (2013.01); H01L 21/02488 (2013.01); H01L 21/02527 (2013.01); H01L 21/02658 (2013.01); H01L 29/1606 (2013.01); H01L 29/82 (2013.01);
Abstract

Direct growth of graphene on CoO(111) at 1000 K was achieved by molecular beam epitaxy from a graphite source. Auger spectroscopy shows a characteristic spcarbon lineshape, at average carbon coverages from 0.4-3 monolayers. Low energy electron diffraction (LEED) indicates (111) ordering of the spcarbon film with a lattice constant of 2.5 (±0.1) Å characteristic of graphene. Six-fold symmetry of the graphene diffraction spots is observed at 0.4, 1 and 3 monolayers. The LEED data also indicate an average domain size of ˜1800 Å, and show an incommensurate interface with the CoO(111) substrate, where the latter exhibits a lattice constant of 2.8 (±0.1) Å. Core level photoemission shows a characteristically asymmetric C(1s) feature, with the expected lr to lr* satellite feature, but with a binding energy for the three monolayer film of 284.9 (±0.1) eV, indicative of substantial graphene-to-oxide charge transfer.


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