The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Apr. 04, 2017
Filed:
Mar. 20, 2014
Nutrichem Company Limited, Beijing, CN;
Shangyu Nutrichem Co., Ltd., Zhejiang, CN;
Wenjun Wang, Beijing, CN;
Jianwei Chen, Beijing, CN;
Jianhong Chi, Beijing, CN;
Yongchang Zhao, Beijing, CN;
Xufang Deng, Beijing, CN;
Long Wang, Beijing, CN;
Hua'nan You, Beijing, CN;
Nutrichem Company Limited, Beijing, CN;
Shanqyu Nutrichem Co., Ltd., Shangyu, CN;
Abstract
Disclosed in the present invention is a preparation method of azoxystrobin having a structure as shown by formula (1), the method comprising: a) performing an etherification reaction by reacting the compound having a structure shown by formula (2) with 2-cyanophenol and/or a salt thereof under the catalysis of an azabicyclo tertiary amine compound and/or a salt thereof as the catalyst in a butyl acetate medium to obtain a butyl acetate solution containing azoxystrobin; and b) cooling the butyl acetate solution containing azoxystrobin to precipitate Azoxystrobin having a structure as shown by formula (1) from the butyl acetate solution. Using the method provided by the present invention to prepare azoxystrobin can significantly improve the yield of azoxystrobin, and can obtain azoxystrobin products having high purity.