The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 28, 2017

Filed:

Jan. 22, 2014
Applicants:

Bruker Biospin Corporation, Billerica, MA (US);

Millikelvin Technologies Llc, Braintree, MA (US);

Inventors:

James G. Kempf, Arlington, MA (US);

Neal Kalechofsky, Stow, MA (US);

Melanie Rosay, Bedford, MA (US);

Assignees:

Bruker Biospin Corporation, Billerica, MA (US);

Millikelvin Technologies LLC, Braintree, MA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G01V 3/00 (2006.01); G01R 33/31 (2006.01); G01R 33/28 (2006.01);
U.S. Cl.
CPC ...
G01R 33/31 (2013.01); G01R 33/282 (2013.01);
Abstract

A method of providing a material sample in a state favorable to retaining spin polarization includes cooling a material sample from a temperature above a freezing point of the material sample down to a second temperature below the freezing point of the material sample; maintaining the sample at about the second temperature for a period of about several hours; and reducing temperature of the material sample to a third temperature lower than the second temperature to provide the material sample in a state favorable to retaining spin polarization, where the steps of cooling, maintaining and reducing are performed in the absence of an adulterant material. The method of providing a sample of pyruvic acid in a state favorable to retaining spin polarization may include cooling the sample of pyruvic acid in the absence of an adulterant material from a temperature above a freezing point of the sample of pyruvic acid down to less than about 200 Kelvin to provide the sample.


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