The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 21, 2017

Filed:

Dec. 17, 2013
Applicant:

Umicore, Brussels, BE;

Inventors:

Stijn Put, Olmen, BE;

Jean-Sebastien Bridel, Geel, BE;

Hailei Zhao, Hebei, CN;

Jing Wang, Hebei, CN;

Assignee:

Umicore, Brussels, BE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
H01M 6/14 (2006.01); H01M 4/36 (2006.01); H01M 10/0525 (2010.01); H01M 4/38 (2006.01); H01M 4/485 (2010.01); H01M 4/587 (2010.01); H01M 4/62 (2006.01); H01M 10/052 (2010.01); H01M 4/02 (2006.01);
U.S. Cl.
CPC ...
H01M 4/364 (2013.01); H01M 4/386 (2013.01); H01M 4/485 (2013.01); H01M 4/587 (2013.01); H01M 4/624 (2013.01); H01M 10/052 (2013.01); H01M 10/0525 (2013.01); H01M 2004/027 (2013.01); Y02E 60/122 (2013.01);
Abstract

The invention relates to a negative electrode powder for a lithium-ion rechargeable battery comprising a mixture comprising carbon and SiO, with 0<x<1, wherein the SiOconsists of a nanometric composite of crystalline SiOand amorphous Si. The method for preparing the powder comprises the steps of providing an aqueous solution comprising an anti-agglomeration agent, dispersing a silicon comprising organic compound in the aqueous solution, hydrothermally treating the aqueous solution at a temperature between 90 and 180° C. for a period of 0.5 to 24 h, preferably between 110 and 140° C. for a period of 0.5 to 4 h, thereby forming a suspension of SiOand Si in the aqueous solution, evaporating the solution, thereby obtaining a slurry, subjecting the slurry to a coking process whereby a solid residue is formed, calcining the solid residue at a temperature between 500 and 1300° C., preferably between 600 and 1000° C., in a non-oxidizing atmosphere.


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