The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 21, 2017

Filed:

Dec. 06, 2013
Applicants:

Tsi (China) Co, Ltd, Shanghai, CN;

Tsi Pharmaceutical (Ji-angyin) Co., Ltd, Jiangsu, CN;

Inventors:

Ling Long, Shanghia, CN;

Yongehun Tang, Jiangsu, CN;

Assignee:

Other;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 51/42 (2006.01); C07C 51/29 (2006.01);
U.S. Cl.
CPC ...
C07C 51/42 (2013.01); C07C 51/29 (2013.01);
Abstract

The present invention relates generally to the field of chemical synthesis. Specifically, the present invention relates to a method for purification of β-hydroxyl-β-methyl butyrate comprising (1) neutralizing a crude β-hydroxyl-β-methyl butyrate; (2) cooling and crystallizing the crude β-hydroxyl-β-methyl butyrate solution to create a β-hydroxyl-β-methyl butyrate salt; (3) dissolving and acidifying the salt; and (4) extracting the resultant high purity β-hydroxyl-β-methyl butyrate. Additionally, the present invention relates to a method of obtaining high purity β-hydroxyl-β-methyl butyrate at normal temperature and vacuum conditions.


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