The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 14, 2017

Filed:

Feb. 11, 2014
Applicants:

Wanhua Chemical (Beijing) Co., Ltd., Beijing, CN;

Wanhua Chemical Group Co., Ltd., Yantai, Shandong, CN;

Wanhua Chemical (Ningbo) Co., Ltd., Ningbo, Zhejiang, CN;

Inventors:

Xiao Zhang, Shandong, CN;

Yulin Zhu, Shandong, CN;

Zhenguang Wen, Shandong, CN;

Kai Wang, Shandong, CN;

Attorney:
Int. Cl.
CPC ...
C07D 251/32 (2006.01); C07D 251/34 (2006.01); C08G 18/79 (2006.01); C08G 18/02 (2006.01); C08G 18/09 (2006.01);
U.S. Cl.
CPC ...
C07D 251/34 (2013.01); C08G 18/022 (2013.01); C08G 18/092 (2013.01);
Abstract

The present invention relates to a method for preparing TDI (toluene diisocyanate) isocyanurate by using TDI, monohydric alcohol, solvent, antioxidant, catalyst and termination agent as the raw materials. The properties of the isocyanurate are improved by the process comprising the modification by monohydric alcohol and addition of the catalyst and solvent in several stages at an appropriate temperature. By adding the catalyst and solvent in batches at the condition of controlling both NCO % and the viscosity in the preparation process, and adjusting the solid content at each step, the resulting TDI isocyanurate has low content of free TDI, high xylene tolerance, small product color number, and high performance stability, which makes the product obtained by the isocyanurate have good application properties such as the drying, polishing and extinction properties of coating film, and such isocyanurate has good compatibility with other components.


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