The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 28, 2017

Filed:

Oct. 22, 2014
Applicants:

Rahul Shankar Bhaduri, Moraga, CA (US);

Hye Kyung Cho Timken, Albany, CA (US);

Philip Ian Cuspard, Danville, CA (US);

Inventors:

Rahul Shankar Bhaduri, Moraga, CA (US);

Hye Kyung Cho Timken, Albany, CA (US);

Philip Ian Cuspard, Danville, CA (US);

Assignee:

Chevron U.S.A. Inc., San Ramon, CA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C22B 11/00 (2006.01); C22B 3/00 (2006.01); B01J 38/64 (2006.01); B01J 38/68 (2006.01); B01J 23/96 (2006.01); B01J 19/18 (2006.01); C22B 7/00 (2006.01); B01J 38/10 (2006.01); B01J 27/13 (2006.01); B01J 27/32 (2006.01);
U.S. Cl.
CPC ...
C22B 11/048 (2013.01); B01J 19/18 (2013.01); B01J 23/96 (2013.01); B01J 38/64 (2013.01); B01J 38/68 (2013.01); C22B 7/009 (2013.01); B01J 27/13 (2013.01); B01J 27/32 (2013.01); B01J 38/10 (2013.01); B01J 2219/00177 (2013.01);
Abstract

A process is provided for preparing a spent noble metal fixed-bed catalyst for precious metals recovery, comprising: a) adding the catalyst to a caustic solution to wash the spent catalyst and to make a wash slurry having an alkaline pH, wherein the spent catalyst has been in contact with chloroaluminate ionic liquid catalyst, and wherein the spent catalyst comprises from 5 to 35 wt % chloride; and b) filtering the wash slurry and collecting: i) a filter cake having from at least 70 wt % of the chloride in the spent catalyst removed and having the noble metals retained, and ii) a wash filtrate. Also provided is a filter cake comprising a washed consolidated cake having 40 to 75 wt % solids, a cake moisture content from 25 to less than 60 wt %, 0.1 to 1.5 wt % total noble metals, and a residual chloride content of from zero to less than 4 wt %.


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