The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 21, 2017

Filed:

Mar. 20, 2014
Applicants:

Corrosion Y Proteccion SA DE Cv, Cuernavaca Morelos, MX;

Universidad Nacional Autonoma DE Mexico, Coyoacan, Mexico City, MX;

Inventors:

Jose Ignacio Regla Contreras, Benito Juarez, MX;

Maria Patricia Shirley Demare Negrete, Mexico City, MX;

Jorge Antonio Ascencio Gutierrez, Cuernavaca Morelos, MX;

Lorenzo Martinez Gomez, Cuernavaca Morelos, MX;

Lorenzo Martinez Martinez De La Escalera, Mexico City, MX;

Jorge Joaquin Canto Ibanez, Mexico City, MX;

Irene Carrillo Salgado, Boca del rio Veracruz, MX;

Assignees:

CORROSION Y PROTECCION SE DE CV, Cuernavaca Morelos, MX;

UNIVERSIDAD NACIONAL AUTONOMA DE MEXICO, Coyoacan, Mexico City, MX;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 233/06 (2006.01); C07D 233/14 (2006.01); C23F 11/14 (2006.01); C05F 5/00 (2006.01);
U.S. Cl.
CPC ...
C07D 233/06 (2013.01); C05F 5/006 (2013.01); C07D 233/14 (2013.01); C23F 11/149 (2013.01); Y02E 50/343 (2013.01); Y02W 30/47 (2015.05);
Abstract

The biphasic extraction from coffee waste without a prior drying process, to obtain coffee oil, which is transesterified with KOH catalyzed methanol to produce mixtures of glycerol free methylic esters, also known as coffee oil biodiesel, which is subjected to an aminolysis reaction with aminoethylethanolamine (AEEA) by heating to 140-160° C. at atmospheric pressure with a subsequent dehydration reaction at the same temperature but at a reduced pressure of 200 to 300 mmHg, in order to achieve cyclization of the intermediary amides into the corresponding imidazolines. Alternatively process, coffee oil can be submitted to the same aminolysis procedure with aminoethylethanolamine (AEEA) at 140 to 160° C. and atmospheric pressure with a subsequent dehydration reaction at the same temperature but at a reduced pressure of 200 to 300 mmHg, to produce imidazolines that contain the residual glycerol of the original triglycerides.


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