The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 21, 2017

Filed:

Sep. 13, 2012
Applicants:

Takehiro Chaki, Settsu, JP;

Kazuhiro Takahashi, Settsu, JP;

Hitoshi Yoshimi, Settsu, JP;

Yoshinori Tanaka, Settsu, JP;

Yuusuke Iwanaga, Settsu, JP;

Inventors:

Takehiro Chaki, Settsu, JP;

Kazuhiro Takahashi, Settsu, JP;

Hitoshi Yoshimi, Settsu, JP;

Yoshinori Tanaka, Settsu, JP;

Yuusuke Iwanaga, Settsu, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 17/38 (2006.01); C07C 17/383 (2006.01); C07C 17/20 (2006.01); C07C 17/25 (2006.01);
U.S. Cl.
CPC ...
C07C 17/383 (2013.01); C07C 17/206 (2013.01); C07C 17/25 (2013.01); C07C 17/38 (2013.01); Y02P 20/582 (2015.11);
Abstract

The present invention provides a method for purifying chlorinated hydrocarbon(s), comprising cooling a mixture containing hydrogen fluoride and at least one chlorinated hydrocarbon selected from the group consisting of 2-chloro-3,3,3-trifluoropropene, 2,3-dichloro-3,3-difluoropropene, 1,2,3-trichloro-1,1-difluoropropane, and 1,1,1,2,3-pentachloropropane to cause liquid-liquid separation of the mixture into an upper liquid phase having a high hydrogen fluoride concentration and a lower liquid phase having a high chlorinated hydrocarbon concentration, and a method for purifying a chlorinated hydrocarbon, comprising subjecting the lower liquid phase obtained by the liquid-liquid separation to a distillation operation. According to the present invention, a chlorinated hydrocarbon can be purified by separating and removing hydrogen fluoride from a chlorinated hydrocarbon-hydrogen fluoride mixture under simple and economically advantageous conditions.


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