The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 27, 2016

Filed:

Jul. 25, 2014
Applicant:

Weylchem Frankfurt Gmbh, Frankfurt Griesheim, DE;

Inventors:

Klaus Forstinger, Babenhausen, DE;

Reinhard Schwesinger, Merzhausen, DE;

Andreas Maier, Eppstein, DE;

Assignee:

WEYLCHEM FRANKFURT GMBH, Frankfurt Griesheim, DE;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 37/00 (2006.01); C07C 37/045 (2006.01); C07C 51/367 (2006.01); C07C 51/00 (2006.01);
U.S. Cl.
CPC ...
C07C 37/00 (2013.01); C07C 37/045 (2013.01); C07C 51/00 (2013.01); C07C 51/367 (2013.01);
Abstract

The present invention relates to a method for the preparation of phenols, in which an aryldiazonium salt, which is prepared by the diazotisation of a corresponding aromatic, primary amine, is decomposed by heating in a mixture containing hot water, a mineral acid and an organic solvent, wherein the organic solvent contains a ketone of formula (I) RC(O)R in which Rand Rindependently stand for (C-C)-alkyl and Rand Rtogether have at least four carbon atoms, wherein the aromatic primary amine is aniline or a substituted aniline, which contains at least one further substituent which is selected from: alkyl, alkenyl, alkynyl, halogen, haloalkyl, cycloalkyl, heteroaryl, carboxyl, cyan, alkoxyl and ester, and wherein substantially no copper salts are contained in the mixture.


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