The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 11, 2016

Filed:

Jun. 06, 2014
Applicant:

Exxonmobil Chemical Patents Inc., Baytown, TX (US);

Inventors:

Jason D. Davis, Beaumont, TX (US);

Christopher L. Becker, Manhattan, KS (US);

Travis A. Reine, Slidell, LA (US);

Bryan A. Patel, Jersey City, NJ (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 45/53 (2006.01); C07C 37/08 (2006.01); C07C 407/00 (2006.01); C07C 29/132 (2006.01);
U.S. Cl.
CPC ...
C07C 407/00 (2013.01); C07C 29/132 (2013.01); C07C 37/08 (2013.01); C07C 45/53 (2013.01); C07C 407/003 (2013.01); C07C 2101/14 (2013.01);
Abstract

Method for concentrating an organic hydroperoxide mixture comprising a hydrocarbon and a hydroperoxide corresponding thereto comprises evaporating a first liquid mixture in a thin-film evaporation device followed by separation in a separation zone. Both the evaporation device and the separation zone operate at a low absolute pressure at a temperature lower than the thermal degradation temperature of the hydroperoxide to prevent thermal decomposition thereof. The process is particularly useful for concentrating an oxidation product made from the oxidation of cyclohexylbenzene.


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