The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 06, 2016

Filed:

Jan. 28, 2015
Applicant:

Battelle Memorial Institute, Richland, WA (US);

Inventors:

Michael A. Lilga, Richland, WA (US);

John G. Frye, Jr., Richland, WA (US);

Suh-Jane Lee, Richland, WA (US);

Karl O. Albrecht, Richland, WA (US);

Assignee:

Battelle Memorial Institute, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 1/24 (2006.01); C07C 29/60 (2006.01); B01J 19/00 (2006.01); C07C 1/207 (2006.01); C07C 49/203 (2006.01); C07C 1/30 (2006.01);
U.S. Cl.
CPC ...
C07C 1/24 (2013.01); B01J 19/00 (2013.01); C07C 29/60 (2013.01); C07C 1/2078 (2013.01); C07C 1/30 (2013.01); C07C 49/203 (2013.01); C07C 2521/04 (2013.01); C07C 2521/06 (2013.01); C07C 2523/02 (2013.01); C07C 2523/08 (2013.01); C07C 2523/10 (2013.01); C07C 2527/167 (2013.01); C07C 2529/40 (2013.01); C07C 2529/70 (2013.01);
Abstract

A composition comprising 2,3-butanediol is dehydrated to methyl vinyl carbinol and/or 1,3-butadiene by exposure to a catalyst comprising (a) MOwherein M is a rare earth metal, a group IIIA metal, Zr, or a combination thereof, and x and y are based upon an oxidation state of M, or (b) M(PO)where Mis a group IA, a group IIA metal, a group IIIA metal, or a combination thereof, and a and b are based upon the oxidation state of M. Embodiments of the catalyst comprising MOmay further include M, wherein Mis a rare earth metal, a group IIA metal, Zr, Al, or a combination thereof. In some embodiments, 2,3-butanediol is dehydrated to methyl vinyl carbinol and/or 1,3-butadiene by a catalyst comprising MO, and the methyl vinyl carbinol is subsequently dehydrated to 1,3-butadiene by exposure to a solid acid catalyst.


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