The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 06, 2016

Filed:

Jan. 22, 2015
Applicant:

Lyondell Chemical Technology, L.p., Houston, TX (US);

Inventors:

Roger Grey, West Chester, PA (US);

Debra Jackson, Huffman, TX (US);

Daniel F. White, Houston, TX (US);

Sandor Nagy, Naperville, TX (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 301/03 (2006.01); B01J 21/08 (2006.01); B01J 37/08 (2006.01); B01J 21/06 (2006.01); B01J 35/10 (2006.01); B01J 37/02 (2006.01); B01J 37/06 (2006.01); B01J 29/03 (2006.01); B01J 29/89 (2006.01); C07D 301/12 (2006.01); C07D 301/19 (2006.01);
U.S. Cl.
CPC ...
B01J 21/08 (2013.01); B01J 21/06 (2013.01); B01J 29/0308 (2013.01); B01J 29/89 (2013.01); B01J 35/10 (2013.01); B01J 37/02 (2013.01); B01J 37/0203 (2013.01); B01J 37/06 (2013.01); B01J 37/08 (2013.01); C07D 301/12 (2013.01); C07D 301/19 (2013.01); B01J 2229/32 (2013.01);
Abstract

A method of preparing epoxidation catalysts is disclosed. The method comprises: (a) adding an inorganic siliceous solid to a column to produce a solid-filled column; (b) adding to the solid-filled column a solution comprising titanium tetrachloride and a hydrocarbon solvent to produce a titanium tetrachloride-impregnated solid; and (c) calcining the titanium tetrachloride-impregnated solid at a temperature from 500° C. to 1000° C. to produce the catalyst. The inorganic siliceous solid has a pore volume of at least 0.8 cm/g.


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