The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 09, 2016

Filed:

Jul. 14, 2011
Applicants:

Mahendra Kumar Sunkara, Louisville, KY (US);

Vivekanand Kumar, Louisville, KY (US);

Jeong H. Kim, Louisville, KY (US);

Ezra Lee Clark, Louisville, KY (US);

Inventors:

Mahendra Kumar Sunkara, Louisville, KY (US);

Vivekanand Kumar, Louisville, KY (US);

Jeong H. Kim, Louisville, KY (US);

Ezra Lee Clark, Louisville, KY (US);

Assignee:
Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01G 23/047 (2006.01); B01J 19/08 (2006.01); B82Y 30/00 (2011.01); B82Y 40/00 (2011.01); C01B 33/32 (2006.01); C30B 25/10 (2006.01); C30B 29/16 (2006.01); C30B 29/60 (2006.01); C01G 23/00 (2006.01); C01G 41/02 (2006.01); C01G 45/02 (2006.01); C01G 51/04 (2006.01); C01G 1/02 (2006.01); C01G 23/04 (2006.01);
U.S. Cl.
CPC ...
B01J 19/088 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01); C01B 33/32 (2013.01); C01G 1/02 (2013.01); C01G 23/005 (2013.01); C01G 23/047 (2013.01); C01G 41/02 (2013.01); C01G 45/02 (2013.01); C01G 51/04 (2013.01); C30B 25/105 (2013.01); C30B 29/16 (2013.01); C30B 29/60 (2013.01); B01J 2219/0879 (2013.01); C01G 23/04 (2013.01); C01G 23/043 (2013.01); C01P 2002/72 (2013.01); C01P 2002/77 (2013.01); C01P 2004/03 (2013.01); C01P 2004/04 (2013.01); C01P 2004/13 (2013.01); C01P 2004/16 (2013.01);
Abstract

A method of synthesizing a metal oxide nanowire includes the steps of: combining an amount of a transition metal or a transition metal oxide with an amount of an alkali metal compound to produce a mixture; activating a plasma discharge reactor to create a plasma discharge; exposing the mixture to the plasma discharge for a first predetermined time period such that transition metal oxide nanowires are formed; contacting the transition metal oxide nanowires with an acid solution such that an alkali metal ion is exchanged for a hydrogen ion on each of the transition metal oxide nanowires; and exposing the transition metal oxide nanowires to the plasma discharge for a second predetermined time period to thermally anneal the transition metal oxide nanowires. Transition metal oxide nanowires produced using the synthesis methods described herein are also provided.


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